form id="form1" runat="server">
 div>
 asp:FileUpload ID="FileUpload1" runat="server" />
 asp:Button ID="Button1" runat="server" Text="上傳" Width="54px" OnClick="Button1_Click" />
 asp:Label ID="Label1" runat="server" Text="" Style="color: Red">/asp:Label>
 asp:Image runat="server" ID="Image1" Style="z-index: 102; left: 20px; position: absolute;
  top: 49px" Width="73px" />
 /div>
 /form>

using System;
using System.Data;
using System.Configuration;
using System.Web;
using System.Web.Security;
using System.Web.UI;
using System.Web.UI.WebControls;
using System.Web.UI.WebControls.WebParts;
using System.Web.UI.HtmlControls;

namespace Web.File
{
 public partial class WebForm1 : System.Web.UI.Page
 {
 protected void Page_Load(object sender, EventArgs e)
 {

 }
 #region 文件上傳
 /// summary>
 /// 文件上傳
 /// /summary>
 protected void Button1_Click(object sender, EventArgs e)
 {
  if (FileUpload1.FileName == "")
  {
  this.Label1.Text = "上傳文件不能為空";
  return;
  }

  bool fileIsValid = false;
  //如果確認了上傳文件，則判斷文件類型是否符合要求 
  if (this.FileUpload1.HasFile)
  {
  //獲取上傳文件的后綴 
  String fileExtension = System.IO.Path.GetExtension(this.FileUpload1.FileName).ToLower();
  String[] restrictExtension = { ".gif", ".jpg", ".bmp", ".png" };
  //判斷文件類型是否符合要求 
  for (int i = 0; i  restrictExtension.Length; i++)
  {
   if (fileExtension == restrictExtension[i])
   {
   fileIsValid = true;
   }
   //如果文件類型符合要求,調用SaveAs方法實現上傳,并顯示相關信息 
   if (fileIsValid == true)
   {
   //上傳文件是否大于10M
   if (FileUpload1.PostedFile.ContentLength > (10 * 1024 * 1024))
   {
    this.Label1.Text = "上傳文件過大";
    return;
   }
   try
   {
    this.Image1.ImageUrl = "~/File/" + FileUpload1.FileName;
    this.FileUpload1.SaveAs(Server.MapPath("~/File/") + FileUpload1.FileName);
    this.Label1.Text = "文件上傳成功!";
   }
   catch
   {
    this.Label1.Text = "文件上傳失敗！";
   }
   finally
   {

   }
   }
   else
   {
   this.Label1.Text = "只能夠上傳后綴為.gif,.jpg,.bmp,.png的文件";
   }
  }
  }
 }
 #endregion
 }
}

!--因為FileUpload 控件上傳最大為4M,如果要上傳更大文件,改下maxRequestLength的大小-->
configuration>
 system.web>
 compilation debug="true" targetFramework="4.0" />
 httpRuntime requestValidationMode="2.0" maxRequestLength="10485760" executionTimeout="3600" appRequestQueueLimit="10000"/>
 /system.web>
/configuration>